碳化物的製備裝置

專利類型

發明

專利國別 (專利申請國家)

中華民國

專利申請案號

109213672

專利證號

M 607637

專利獲證名稱

碳化物的製備裝置

專利所屬機關 (申請機關)

國立清華大學

獲證日期

2021/02/11

技術說明

本新型提供一種碳化物的製備裝置，其包含槽體、蓋體、熔融鹽坩堝、電極組件、進氣設備以及加熱設備。蓋體與槽體連接並共同界定出一容置空間。熔融鹽坩堝位於容置空間內且用於盛裝一鹽類。電極組件包含工作電極及輔助電極，工作電極與輔助電極的一端均接觸熔融鹽坩堝中的鹽類，且工作電極接觸鹽類的一端係供一反應錠固定。進氣設備用以抽換容置空間中的氣體，而加熱設備用以加熱容置空間。本新型的製備裝置係供含有無定型碳的反應錠與熔融態的鹽類進行電化學反應，以形成碳化物，藉此降低製程複雜度，同時大幅節省能源消耗及生產成本。 A manufacturing apparatus of carbide according to the present disclosure includes a tank, a lid, a molten salt crucible, an electrode assembly, an air intake device and a heating device. The lid is connected to the tank to jointly delimit a compartment. The molten salt crucible is disposed in the compartment and configured to hold a salt. The electrode assembly includes a working electrode and a counter electrode. An end of the working electrode and an end of the counter electrode are both in contact with the salt in the molten salt crucible, and the end of the working electrode in contact with the salt is fixed with a reactant tablet. The air intake device is configured to exchange the air in the compartment. The heating device is configured to heat the compartment. The manufacturing apparatus of the present disclosure is adapted for performing the electrochemical reaction between the reactant tablet with amorphous carbon and the molten salt, so as to form the carbide. In this regard, the complexity of the manufacturing process is decreased, and energy consumption and manufacturing cost are significantly reduced.

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